SYNTHESIS AND CHARACTERIZATION NMR 1D AND 2D OF THE SULPHURATED DERIVATIVES OF THE 1-PHENYL- 3-METHYL-2-PIRAZOLINE-5-ONA AND THEIR LIGAND POTENCIAL CAPACITY
Abstract
In this work the result of the synthesis of the 4- hexil-dithiocarboxilate-1-phenil-3-methyl-
2-pirazolin-5-ona(PirC6), and 4-dithiocarboxilate of dodecil-1-phenil-3-methyl-2-pirazolin-
5-ona(PirC12), is presented and the products are characterized, using the microanalysis ,
the infrared spectroscopy, the spectroscopy of NMR of H1 and C13 and the NMR in two
dimensions (HSQC and HMBC), in order to determine their structures. In addition, the
ligand potential capacity of these products are studied in order to produce coordination
compounds with the uranil (UO2
2+).
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